Solutions Intermediate Students Book Answer Key Download
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The generation of the intermediate magnetic field and the polarization of the nuclear magnetic resonance in the homogeneous magnetic field of the next generation of NMR spectrometers with superconducting magnets was investigated. The values of the intermediate magnetic field were determined by the measurement of the line widths of the proton NMR spectra in aqueous solutions of paramagnetic ions. For efficient relaxation of the nuclear magnetization in the intermediate magnetic field, the creation of the intermediate magnetic field is accomplished using a superconducting solenoid and a permanent magnet. The generation of the intermediate magnetic field in a solution of paramagnetic ions exhibits a number of peculiarities. The contribution of the relaxation of the nuclear magnetization in the intermediate magnetic fields to the total relaxation of the nuclear magnetization is less than 1%, and in some cases even completely negligible. An example of the polarization of nuclear magnetization in the intermediate magnetic field is also presented.
The two-electron relaxation processes in the intermediate magnetic fields are studied. The effective relaxation rate constants are found for the first three triplets. The two-electron relaxation processes are shown to be the primary ones in the intermediate magnetic fields for the first three triplets. However, the two-electron relaxation processes are shown to be suppressed in the intermediate magnetic fields for the last triplet.
One-electron relaxation processes are among the most intensively studied processes in the intermediated magnetic fields. The contribution of the relaxation processes in the intermediate magnetic fields of the first three triplets is presented. This problem was solved using a simple quasi-equilibrium approximation. The obtained results show that the relaxation processes which are dominated by T1 and T2 relaxation are the primary ones in the intermediate magnetic fields for the first three triplets. Moreover, it is shown that under certain conditions the relaxation processes which are dominated by the C--O exchange, C--C exchange, and C--F exchange may be the primary ones in the intermediate magnetic fields for the last triplet (the triplet for which the internal conversion is the dominant relaxation mechanism).
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